An electrochemical quartz crystal microbalance study of lithium insertion into thin films of tungsten trioxide. II: Experimental results and comparison with model calculations
Identifieur interne : 01D012 ( Main/Repository ); précédent : 01D011; suivant : 01D013An electrochemical quartz crystal microbalance study of lithium insertion into thin films of tungsten trioxide. II: Experimental results and comparison with model calculations
Auteurs : RBID : Pascal:95-0555843Descripteurs français
- Pascal (Inist)
- Etude théorique, Etude expérimentale, Etude comparative, Electrode, Indium Oxyde, Etain Oxyde, Matériau modifié, Tungstène VI Oxyde, Couche mince, Matériau amorphe, Lithium Perchlorate, Chronoampérométrie, Voltammétrie cyclique, Microbalance quartz, Réaction électrochimique, Composé insertion, Lithium Ion, Modélisation, Modèle mathématique, Analyse thermodynamique, Coefficient diffusion, Fonction transfert, Mécanisme réaction, Constante vitesse, Paramètre cinétique, Electrode ITO, 1,3-Dioxolan-2-one(méthyl).
- Wicri :
- concept : Matériau amorphe.
English descriptors
- KwdEn :
- Amorphous material, Chronoamperometry, Comparative study, Cyclic voltammetry, Diffusion coefficient, Electrochemical reaction, Electrodes, Experimental study, Indium Oxides, Intercalation compound, Kinetic parameter, Lithium Ions, Lithium Perchlorates, Mathematical model, Modeling, Modified material, Quartz microbalance, Rate constant, Reaction mechanism, Theoretical study, Thermodynamic analysis, Thin film, Tin Oxides, Transfer function, Tungsten VI Oxides.
Abstract
Lithium insertion into amorphous thin films of tungsten trioxide (a-WO3) prepared by thermal vacuum evaporation of WO3 powder has been studied experimentally by chronoamperometry, cyclic voltammetry and ac impedance spectroscopy associated with electrochemical quartz crystal microbalance (EQCM). During cathodic polarization of the electrode and at short times two antagonistic processes occur. One is a non faradaic process and is associated with the expulsion of anions from the electrode surface under the effect of the electric field built in the electrolyte when a potential difference is imposed between the electrodes. The other one is the faradaic insertion of non-solvated lithium ions into the oxide. These two processes occur simultaneously. Under application of a cathodic overvoltage the former one leads to a loss of mass of the electrode and the latter one to a gain of mass. These two processes may explain the experimental data. From these data the diffusion coefficient of lithium ions into the oxide is determined and it is shown that it varies as insertion proceeds. A thermodynamic study of lithium insertion into a-WO3 is also performed to solve the equations of the theoretical model proposed in Part I of this paper. This thermodynamic study allowed us to determine the repulsive and/or attractive interactions between the inserted species and the host matrix as insertion occurs and the influence of the electronic term on the potential.
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<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en" level="a">An electrochemical quartz crystal microbalance study of lithium insertion into thin films of tungsten trioxide. II: Experimental results and comparison with model calculations</title><author><name sortKey="Bohnke, O" uniqKey="Bohnke O">O. Bohnke</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>CNRS Univ. Maine, URA 449 lab. fluorures</s1><s2>72017 Le Mans</s2><s3>FRA</s3><sZ>1 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Pays de la Loire</region><settlement type="city">Le Mans</settlement></placeName></affiliation></author><author><name sortKey="Vuillemin, B" uniqKey="Vuillemin B">B. Vuillemin</name><affiliation wicri:level="3"><inist:fA14 i1="02"><s1>CNRS Univ. Bourgogne, URA 23 lab. rech. réactivité solides</s1><s2>21004 Dijon</s2><s3>FRA</s3><sZ>2 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Bourgogne</region><settlement type="city">Dijon</settlement></placeName></affiliation></author><author><name sortKey="Gabrielli, C" uniqKey="Gabrielli C">C. Gabrielli</name><affiliation wicri:level="3"><inist:fA14 i1="03"><s1>CNRS, UPR 15 physiques électrochimie</s1><s2>Univ. P. et M. Curie, 75252 Paris</s2><s3>FRA</s3><sZ>3 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Île-de-France</region><settlement type="city">Paris</settlement></placeName></affiliation></author><author><name sortKey="Keddam, M" uniqKey="Keddam M">M. Keddam</name><affiliation wicri:level="3"><inist:fA14 i1="03"><s1>CNRS, UPR 15 physiques électrochimie</s1><s2>Univ. P. et M. Curie, 75252 Paris</s2><s3>FRA</s3><sZ>3 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Île-de-France</region><settlement type="city">Paris</settlement></placeName></affiliation></author><author><name sortKey="Perrot, H" uniqKey="Perrot H">H. Perrot</name><affiliation wicri:level="3"><inist:fA14 i1="03"><s1>CNRS, UPR 15 physiques électrochimie</s1><s2>Univ. P. et M. Curie, 75252 Paris</s2><s3>FRA</s3><sZ>3 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Île-de-France</region><settlement type="city">Paris</settlement></placeName></affiliation></author></titleStmt><publicationStmt><idno type="inist">95-0555843</idno><date when="1995">1995</date><idno type="stanalyst">PASCAL 95-0555843 INIST</idno><idno type="RBID">Pascal:95-0555843</idno><idno type="wicri:Area/Main/Corpus">01BB98</idno><idno type="wicri:Area/Main/Repository">01D012</idno></publicationStmt><seriesStmt><idno type="ISSN">0013-4686</idno><title level="j" type="abbreviated">Electrochim. acta</title><title level="j" type="main">Electrochimica acta</title></seriesStmt></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Amorphous material</term><term>Chronoamperometry</term><term>Comparative study</term><term>Cyclic voltammetry</term><term>Diffusion coefficient</term><term>Electrochemical reaction</term><term>Electrodes</term><term>Experimental study</term><term>Indium Oxides</term><term>Intercalation compound</term><term>Kinetic parameter</term><term>Lithium Ions</term><term>Lithium Perchlorates</term><term>Mathematical model</term><term>Modeling</term><term>Modified material</term><term>Quartz microbalance</term><term>Rate constant</term><term>Reaction mechanism</term><term>Theoretical study</term><term>Thermodynamic analysis</term><term>Thin film</term><term>Tin Oxides</term><term>Transfer function</term><term>Tungsten VI Oxides</term></keywords><keywords scheme="Pascal" xml:lang="fr"><term>Etude théorique</term><term>Etude expérimentale</term><term>Etude comparative</term><term>Electrode</term><term>Indium Oxyde</term><term>Etain Oxyde</term><term>Matériau modifié</term><term>Tungstène VI Oxyde</term><term>Couche mince</term><term>Matériau amorphe</term><term>Lithium Perchlorate</term><term>Chronoampérométrie</term><term>Voltammétrie cyclique</term><term>Microbalance quartz</term><term>Réaction électrochimique</term><term>Composé insertion</term><term>Lithium Ion</term><term>Modélisation</term><term>Modèle mathématique</term><term>Analyse thermodynamique</term><term>Coefficient diffusion</term><term>Fonction transfert</term><term>Mécanisme réaction</term><term>Constante vitesse</term><term>Paramètre cinétique</term><term>Electrode ITO</term><term>1,3-Dioxolan-2-one(méthyl)</term></keywords><keywords scheme="Wicri" type="concept" xml:lang="fr"><term>Matériau amorphe</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">Lithium insertion into amorphous thin films of tungsten trioxide (a-WO<sub>3</sub>) prepared by thermal vacuum evaporation of WO<sub>3</sub> powder has been studied experimentally by chronoamperometry, cyclic voltammetry and ac impedance spectroscopy associated with electrochemical quartz crystal microbalance (EQCM). During cathodic polarization of the electrode and at short times two antagonistic processes occur. One is a non faradaic process and is associated with the expulsion of anions from the electrode surface under the effect of the electric field built in the electrolyte when a potential difference is imposed between the electrodes. The other one is the faradaic insertion of non-solvated lithium ions into the oxide. These two processes occur simultaneously. Under application of a cathodic overvoltage the former one leads to a loss of mass of the electrode and the latter one to a gain of mass. These two processes may explain the experimental data. From these data the diffusion coefficient of lithium ions into the oxide is determined and it is shown that it varies as insertion proceeds. A thermodynamic study of lithium insertion into a-WO<sub>3</sub> is also performed to solve the equations of the theoretical model proposed in Part I of this paper. This thermodynamic study allowed us to determine the repulsive and/or attractive interactions between the inserted species and the host matrix as insertion occurs and the influence of the electronic term on the potential.</div></front></TEI><inist><standard h6="B"><pA><fA01 i1="01" i2="1"><s0>0013-4686</s0></fA01><fA02 i1="01"><s0>ELCAAV</s0></fA02><fA03 i2="1"><s0>Electrochim. acta</s0></fA03><fA05><s2>40</s2></fA05><fA06><s2>17</s2></fA06><fA08 i1="01" i2="1" l="ENG"><s1>An electrochemical quartz crystal microbalance study of lithium insertion into thin films of tungsten trioxide. II: Experimental results and comparison with model calculations</s1></fA08><fA11 i1="01" i2="1"><s1>BOHNKE (O.)</s1></fA11><fA11 i1="02" i2="1"><s1>VUILLEMIN (B.)</s1></fA11><fA11 i1="03" i2="1"><s1>GABRIELLI (C.)</s1></fA11><fA11 i1="04" i2="1"><s1>KEDDAM (M.)</s1></fA11><fA11 i1="05" i2="1"><s1>PERROT (H.)</s1></fA11><fA14 i1="01"><s1>CNRS Univ. Maine, URA 449 lab. fluorures</s1><s2>72017 Le Mans</s2><s3>FRA</s3><sZ>1 aut.</sZ></fA14><fA14 i1="02"><s1>CNRS Univ. Bourgogne, URA 23 lab. rech. réactivité solides</s1><s2>21004 Dijon</s2><s3>FRA</s3><sZ>2 aut.</sZ></fA14><fA14 i1="03"><s1>CNRS, UPR 15 physiques électrochimie</s1><s2>Univ. P. et M. Curie, 75252 Paris</s2><s3>FRA</s3><sZ>3 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ></fA14><fA20><s1>2765-2773</s1></fA20><fA21><s1>1995</s1></fA21><fA23 i1="01"><s0>ENG</s0></fA23><fA43 i1="01"><s1>INIST</s1><s2>1516</s2><s5>354000050273630090</s5></fA43><fA44><s0>0000</s0></fA44><fA45><s0>19 ref.</s0></fA45><fA47 i1="01" i2="1"><s0>95-0555843</s0></fA47><fA60><s1>P</s1></fA60><fA61><s0>A</s0></fA61><fA64 i1="01" i2="1"><s0>Electrochimica acta</s0></fA64><fA66 i1="01"><s0>GBR</s0></fA66><fC01 i1="01" l="ENG"><s0>Lithium insertion into amorphous thin films of tungsten trioxide (a-WO<sub>3</sub>) prepared by thermal vacuum evaporation of WO<sub>3</sub> powder has been studied experimentally by chronoamperometry, cyclic voltammetry and ac impedance spectroscopy associated with electrochemical quartz crystal microbalance (EQCM). During cathodic polarization of the electrode and at short times two antagonistic processes occur. One is a non faradaic process and is associated with the expulsion of anions from the electrode surface under the effect of the electric field built in the electrolyte when a potential difference is imposed between the electrodes. The other one is the faradaic insertion of non-solvated lithium ions into the oxide. These two processes occur simultaneously. Under application of a cathodic overvoltage the former one leads to a loss of mass of the electrode and the latter one to a gain of mass. These two processes may explain the experimental data. From these data the diffusion coefficient of lithium ions into the oxide is determined and it is shown that it varies as insertion proceeds. A thermodynamic study of lithium insertion into a-WO<sub>3</sub> is also performed to solve the equations of the theoretical model proposed in Part I of this paper. This thermodynamic study allowed us to determine the repulsive and/or attractive interactions between the inserted species and the host matrix as insertion occurs and the influence of the electronic term on the potential.</s0></fC01><fC02 i1="01" i2="1"><s0>001C01H05</s0></fC02><fC03 i1="01" i2="X" l="FRE"><s0>Etude théorique</s0><s5>01</s5></fC03><fC03 i1="01" i2="X" l="ENG"><s0>Theoretical study</s0><s5>01</s5></fC03><fC03 i1="01" i2="X" l="GER"><s0>Theoretische Untersuchung</s0><s5>01</s5></fC03><fC03 i1="01" i2="X" l="SPA"><s0>Estudio teórico</s0><s5>01</s5></fC03><fC03 i1="02" i2="X" l="FRE"><s0>Etude expérimentale</s0><s5>02</s5></fC03><fC03 i1="02" i2="X" l="ENG"><s0>Experimental study</s0><s5>02</s5></fC03><fC03 i1="02" i2="X" l="GER"><s0>Experimentelle Untersuchung</s0><s5>02</s5></fC03><fC03 i1="02" i2="X" l="SPA"><s0>Estudio experimental</s0><s5>02</s5></fC03><fC03 i1="03" i2="X" l="FRE"><s0>Etude comparative</s0><s5>03</s5></fC03><fC03 i1="03" i2="X" l="ENG"><s0>Comparative 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difusión</s0><s5>22</s5></fC03><fC03 i1="22" i2="X" l="FRE"><s0>Fonction transfert</s0><s5>23</s5></fC03><fC03 i1="22" i2="X" l="ENG"><s0>Transfer function</s0><s5>23</s5></fC03><fC03 i1="22" i2="X" l="GER"><s0>Uebertragungsfunktion</s0><s5>23</s5></fC03><fC03 i1="22" i2="X" l="SPA"><s0>Función traspaso</s0><s5>23</s5></fC03><fC03 i1="23" i2="X" l="FRE"><s0>Mécanisme réaction</s0><s5>24</s5></fC03><fC03 i1="23" i2="X" l="ENG"><s0>Reaction mechanism</s0><s5>24</s5></fC03><fC03 i1="23" i2="X" l="SPA"><s0>Mecanismo reacción</s0><s5>24</s5></fC03><fC03 i1="24" i2="X" l="FRE"><s0>Constante vitesse</s0><s5>25</s5></fC03><fC03 i1="24" i2="X" l="ENG"><s0>Rate constant</s0><s5>25</s5></fC03><fC03 i1="24" i2="X" l="SPA"><s0>Constante velocidad</s0><s5>25</s5></fC03><fC03 i1="25" i2="X" l="FRE"><s0>Paramètre cinétique</s0><s5>26</s5></fC03><fC03 i1="25" i2="X" l="ENG"><s0>Kinetic parameter</s0><s5>26</s5></fC03><fC03 i1="25" i2="X" l="SPA"><s0>Parámetro cinético</s0><s5>26</s5></fC03><fC03 i1="26" i2="X" l="FRE"><s0>Electrode ITO</s0><s4>INC</s4><s5>62</s5></fC03><fC03 i1="27" i2="X" l="FRE"><s0>1,3-Dioxolan-2-one(méthyl)</s0><s1>SOL</s1><s2>NK</s2><s4>INC</s4><s5>63</s5></fC03><fN21><s1>317</s1></fN21></pA></standard></inist></record>Pour manipuler ce document sous Unix (Dilib)
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|type= RBID
|clé= Pascal:95-0555843
|texte= An electrochemical quartz crystal microbalance study of lithium insertion into thin films of tungsten trioxide. II: Experimental results and comparison with model calculations
}}
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